ScholarLens Back to search
2012•Textile Dyeing and Finishing JournalRequires access

Study on the synthesis of ester containing asymmetric cationic surfactant

Tong Bai

Open publisher page 0 citations

Abstract

The intermediate N,N-dimethylaminoethyl benzoate(Ⅰ) was synthesized from dimethyl phthalate ester, N,N-dimethyl ethanolamine catalyzed by sodium methoxide-methanol solution by transestenfication.The yield ofⅠis 24.90%.Ester containing asymmetric cationic surfactant(Ⅱ) was synthesized with the N,N-dimethylaminoethyl phthalate ester and 1-bromooctane by quaternization.The yield ofⅡis 51.61%.The optimum conditions were investigated by single factor experimental.The structures of intermediate and product are verified by ~1H-NMR and IR.

About this research paper

What this paper is about

The intermediate N,N-dimethylaminoethyl benzoate(Ⅰ) was synthesized from dimethyl phthalate ester, N,N-dimethyl ethanolamine catalyzed by sodium methoxide-methanol solution by transestenfication.The yield ofⅠis 24.90%.Ester containing asymmetric cationic surfactant(Ⅱ) was synthesized with the N,N-dimethylaminoethyl phthalate ester and 1-bromooctane by quaternization.The yield ofⅡis 51.61%.The optimum conditions were investigated by single factor experimental.The structures of intermediate and product are verified by ~1H-NMR and IR.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

The intermediate N,N-dimethylaminoethyl benzoate(Ⅰ) was synthesized from dimethyl phthalate ester, N,N-dimethyl ethanolamine catalyzed by sodium methoxide-methanol solution by transestenfication.The yield ofⅠis 24.90%.Ester containing asymmetric cationic surfactant(Ⅱ) was synthesized with the N,N-dimethylaminoethyl phthalate ester and 1-bromooctane by quaternization.The yield ofⅡis 51.61%.The optimum conditions were investigated by single factor experimental.The structures of intermediate and product are verified by ~1H-NMR and IR.

Key concepts: Sodium methoxide, Cationic polymerization, Pulmonary surfactant, Yield (engineering), Methanol, Ethanolamine, Chemistry, Dimethyl phthalate

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Study on the synthesis of ester containing asymmetric cationic surfactant — Research Paper | ScholarLens