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Synthesis,Characterization and Crystal Structure of One-dimensional Chainlike Ag(I) Coordination Polymer

Huang Yan

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Abstract

One coordination polymer [Ag 2(L)(LH)]NO 3 ·1.5H 2 O(1,LH =2-(4-methoxyphenyl)-1H-imidazo phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectrum,TG and single-crystal X-ray diffraction.Complex 1 crystallizes in the monoclinic system,space group C2/c,with a=2.733 8(6),b=1.580 7(3),c=1.736 0(4) nm,β=107.73(3)°,V=7.146(2) nm 3,Z=4,293(2) K.In the crystal structure,two Ag ions are three match coordination with three nitrogen atoms from different LH and L ligands,assuming a slightly distorted triangle,respectively.

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What this paper is about

One coordination polymer [Ag 2(L)(LH)]NO 3 ·1.5H 2 O(1,LH =2-(4-methoxyphenyl)-1H-imidazo phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectrum,TG and single-crystal X-ray diffraction.Complex 1 crystallizes in the monoclinic system,space group C2/c,with a=2.733 8(6),b=1.580 7(3),c=1.736 0(4) nm,β=107.73(3)°,V=7.146(2) nm 3,Z=4,293(2) K.In the crystal structure,two Ag ions are three match coordination with three nitrogen atoms from different LH and L ligands,assuming a slightly distorted triangle,respectively.

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Available abstract

One coordination polymer [Ag 2(L)(LH)]NO 3 ·1.5H 2 O(1,LH =2-(4-methoxyphenyl)-1H-imidazo phenanthroline) has been hydrothermally synthesized and structurally characterized by elemental analysis,IR spectrum,TG and single-crystal X-ray diffraction.Complex 1 crystallizes in the monoclinic system,space group C2/c,with a=2.733 8(6),b=1.580 7(3),c=1.736 0(4) nm,β=107.73(3)°,V=7.146(2) nm 3,Z=4,293(2) K.In the crystal structure,two Ag ions are three match coordination with three nitrogen atoms from different LH and L ligands,assuming a slightly distorted triangle,respectively.

Key concepts: Monoclinic crystal system, Crystallography, Coordination polymer, Crystal structure, Ion, Elemental analysis, Chemistry, Single crystal

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