Catalytic synthesis of dibutyl succinate with sodium bisulfate
Zi Jun
Abstract
Zi Jun
Abstract
Dibutyl succinate is synthesized from succinic acid and nbutyl alcohol with sodium bisulfate as catalyst. The effects of factors on esterification ratio are studied. The best reaction conditions are as follows: based on 0.05?mol succinic acid, the molar ratio of nbutyl alcohol to succinic acid is 2.5, mass of catalyst is 0.12?g, the taking water reagent is 5?ml, and the reaction time is 30?min. The esterification ratio is over 98%. The experimental results show that sodium bisulfate is an excellent catalyst for synthesis of dibutyl succinate.
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Dibutyl succinate is synthesized from succinic acid and nbutyl alcohol with sodium bisulfate as catalyst. The effects of factors on esterification ratio are studied. The best reaction conditions are as follows: based on 0.05?mol succinic acid, the molar ratio of nbutyl alcohol to succinic acid is 2.5, mass of catalyst is 0.12?g, the taking water reagent is 5?ml, and the reaction time is 30?min. The esterification ratio is over 98%. The experimental results show that sodium bisulfate is an excellent catalyst for synthesis of dibutyl succinate.
Key concepts: Succinic acid, Chemistry, Catalysis, Alcohol, Reagent, Molar ratio, Sodium, Nuclear chemistry