DETERMINATION OF AS,SB AND BI IN COPPER CONCENTRATES BY HYDRIDE GENERATION ATOMIC FLUORESCENCE SPECTROMETRY
Sun Jian-wen
Abstract
Sun Jian-wen
Abstract
The major-element matching method was used to eliminate matrix interference.Experimental conditions including acid degree and reducing agent concentration were optimized,Good linear relations with fluorescence strength were obtained for As,Sb,Bi in the concentration ranging from 1 to 200μg·L-1.Recovery rates from 92% to 101% were achieved with relative standard deviation ranging from 2.7% to 5.5%.
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The major-element matching method was used to eliminate matrix interference.Experimental conditions including acid degree and reducing agent concentration were optimized,Good linear relations with fluorescence strength were obtained for As,Sb,Bi in the concentration ranging from 1 to 200μg·L-1.Recovery rates from 92% to 101% were achieved with relative standard deviation ranging from 2.7% to 5.5%.
Key concepts: Relative standard deviation, Hydride, Copper, Analytical Chemistry (journal), Ranging, Chemistry, Mass spectrometry, Fluorescence