2003Hecheng huaxueRequires access

Synthesis of Amyl Butyrate in Liquid-Solid Phase Using β Zeolites as Catalysts

Long Li

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Abstract

βZeolites were used as catalysts for the esterification reaction of n-butyric acid with n-amyl alcohol in liquid-solid phase. The effects of the amount of the catalyst, and the type of the cation in β zeolite, the ratio of reactants, reaction time, the amount of cyclohexane, and the activation time of the catalyst on the conversion of n-butyric acid and the yield of amyl butyrate were investigated. The kinetic equations for the noncatalytic esterification and those of the esterification with Al-β zeolite as a catalyst were established.

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What this paper is about

βZeolites were used as catalysts for the esterification reaction of n-butyric acid with n-amyl alcohol in liquid-solid phase. The effects of the amount of the catalyst, and the type of the cation in β zeolite, the ratio of reactants, reaction time, the amount of cyclohexane, and the activation time of the catalyst on the conversion of n-butyric acid and the yield of amyl butyrate were investigated. The kinetic equations for the noncatalytic esterification and those of the esterification with Al-β zeolite as a catalyst were established.

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Available abstract

βZeolites were used as catalysts for the esterification reaction of n-butyric acid with n-amyl alcohol in liquid-solid phase. The effects of the amount of the catalyst, and the type of the cation in β zeolite, the ratio of reactants, reaction time, the amount of cyclohexane, and the activation time of the catalyst on the conversion of n-butyric acid and the yield of amyl butyrate were investigated. The kinetic equations for the noncatalytic esterification and those of the esterification with Al-β zeolite as a catalyst were established.

Key concepts: Chemistry, Catalysis, Zeolite, Yield (engineering), Cyclohexane, Alcohol, Organic chemistry, Butyric acid

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