2008Unpublished venueRequires access

Study on the Analysis of 70 Pesticides in Fruits and Vegetables Using Liquid Chromatography with Tandem Mass Spectrometric Detection

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Abstract

A multi-residue method for the determination of 70 pesticides in fruits and veg- etables by means of LC-MS/MS is presented.The pesticides were extracted by acetonitrile,pu- rified using SPE and finally detected by LC-MS/MS within 35 minutes.The method is proved to be linear obtaining correlation coefficients from 0.995 to 1.000 over the range 0.01~2.00 μg/mL.The obtained recoveries are in the range 70%~120% and the LOD is 10 μg/kg.The LOD,recovery and RSD can meet the demands of the analysis of pesticide residue.

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A multi-residue method for the determination of 70 pesticides in fruits and veg- etables by means of LC-MS/MS is presented.The pesticides were extracted by acetonitrile,pu- rified using SPE and finally detected by LC-MS/MS within 35 minutes.The method is proved to be linear obtaining correlation coefficients from 0.995 to 1.000 over the range 0.01~2.00 μg/mL.The obtained recoveries are in the range 70%~120% and the LOD is 10 μg/kg.The LOD,recovery and RSD can meet the demands of the analysis of pesticide residue.

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Available abstract

A multi-residue method for the determination of 70 pesticides in fruits and veg- etables by means of LC-MS/MS is presented.The pesticides were extracted by acetonitrile,pu- rified using SPE and finally detected by LC-MS/MS within 35 minutes.The method is proved to be linear obtaining correlation coefficients from 0.995 to 1.000 over the range 0.01~2.00 μg/mL.The obtained recoveries are in the range 70%~120% and the LOD is 10 μg/kg.The LOD,recovery and RSD can meet the demands of the analysis of pesticide residue.

Key concepts: Chromatography, Residue (chemistry), Pesticide, Chemistry, Pesticide residue, Liquid chromatography–mass spectrometry, Tandem mass spectrometry, Linear range

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