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SYNTHESIS OF N-AMYL CINNAMATE BY USING TiSiW_(12)O_(40)/TiO_2 AS CATALYST

Bin Hu

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Abstract

The synthesis n amyl cinnamate of using TiSiW 12 O 40 /TiO 2 as catalyst has been studied. The factors influencing the synthesis were discussed and the best conditions were found out. The optimum conditions are: molar ratio of n amyl alcohol to cinnamic acid is 4∶1,the quantity of catalyst is equal to 2.0% feed stock, the reaction temperature is 122?℃-126?℃, and the reaction time is 1.5?h. TiSiW 12 O 40 /TiO 2 is an excellent catalyst for synthetizing n amyl cinnamate and its yield can reach over 93.33%.

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What this paper is about

The synthesis n amyl cinnamate of using TiSiW 12 O 40 /TiO 2 as catalyst has been studied. The factors influencing the synthesis were discussed and the best conditions were found out. The optimum conditions are: molar ratio of n amyl alcohol to cinnamic acid is 4∶1,the quantity of catalyst is equal to 2.0% feed stock, the reaction temperature is 122?℃-126?℃, and the reaction time is 1.5?h. TiSiW 12 O 40 /TiO 2 is an excellent catalyst for synthetizing n amyl cinnamate and its yield can reach over 93.33%.

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Available abstract

The synthesis n amyl cinnamate of using TiSiW 12 O 40 /TiO 2 as catalyst has been studied. The factors influencing the synthesis were discussed and the best conditions were found out. The optimum conditions are: molar ratio of n amyl alcohol to cinnamic acid is 4∶1,the quantity of catalyst is equal to 2.0% feed stock, the reaction temperature is 122?℃-126?℃, and the reaction time is 1.5?h. TiSiW 12 O 40 /TiO 2 is an excellent catalyst for synthetizing n amyl cinnamate and its yield can reach over 93.33%.

Key concepts: Catalysis, Molar ratio, Yield (engineering), Alcohol, Chemistry, Organic chemistry, Nuclear chemistry, Materials science

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