Determination of Cadmium in Grain by FAAS with Microwave Digestion
Liu Jian
Abstract
Liu Jian
Abstract
This article used the method of microwave digestion-flame atomic absorption spectrometry(FAAS) to determine cadmium in grain.The digestion plan and the parameters of FAAS were optimized and selected.The linear range was 0—8.0mg ? L~(-1),the detection limit was 1.7μg ? L~(-1),and the recovery rate was 95.0%—106.7%.This method is simple,fast,with less reagent consumption and good reproducibility.
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This article used the method of microwave digestion-flame atomic absorption spectrometry(FAAS) to determine cadmium in grain.The digestion plan and the parameters of FAAS were optimized and selected.The linear range was 0—8.0mg ? L~(-1),the detection limit was 1.7μg ? L~(-1),and the recovery rate was 95.0%—106.7%.This method is simple,fast,with less reagent consumption and good reproducibility.
Key concepts: Microwave digestion, Digestion (alchemy), Detection limit, Reproducibility, Cadmium, Reagent, Chemistry, Analytical Chemistry (journal)