2013•Trace Elements ScienceRequires access

Determination of Benzene Series in Adhesives by Gas Chromatography with Headspace-Direct Injection Method

XU Jianing

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Abstract

Objective Establish the method for the determination of benzene,toluene,ethyl benzene,xylene,benzene,xylene and styrene(7 analytes) in adhesives by gas chromatography with headspace-direct injection.Method The column in gas chromatography,the heating temperature of headspace and headspace extraction time were discussed.Result 7 analytes detection limits are less than 5 mg/kg,7 kinds of components in a capillary column can be separated well,the recovery rate is in the range of 81%~94%,RSD is 5% ~ 10%.The method is fast and simple to operate.Conclusion This method is able to meet for determination and analysis requirements of the adhesives of benzene series compounds.

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What this paper is about

Objective Establish the method for the determination of benzene,toluene,ethyl benzene,xylene,benzene,xylene and styrene(7 analytes) in adhesives by gas chromatography with headspace-direct injection.Method The column in gas chromatography,the heating temperature of headspace and headspace extraction time were discussed.Result 7 analytes detection limits are less than 5 mg/kg,7 kinds of components in a capillary column can be separated well,the recovery rate is in the range of 81%~94%,RSD is 5% ~ 10%.The method is fast and simple to operate.Conclusion This method is able to meet for determination and analysis requirements of the adhesives of benzene series compounds.

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Available abstract

Objective Establish the method for the determination of benzene,toluene,ethyl benzene,xylene,benzene,xylene and styrene(7 analytes) in adhesives by gas chromatography with headspace-direct injection.Method The column in gas chromatography,the heating temperature of headspace and headspace extraction time were discussed.Result 7 analytes detection limits are less than 5 mg/kg,7 kinds of components in a capillary column can be separated well,the recovery rate is in the range of 81%~94%,RSD is 5% ~ 10%.The method is fast and simple to operate.Conclusion This method is able to meet for determination and analysis requirements of the adhesives of benzene series compounds.

Key concepts: Benzene, Toluene, Chromatography, Xylene, Gas chromatography, Chemistry, Analyte, Styrene

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