2013•Applied Chemical IndustryRequires access
Synthesis of 5-(2-hydroxyethyl)-2,2-dimethyl-1,3-dioxane
Dawei Teng
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Abstract
5-(2-Hydroxyethyl)-2,2-dimethyl-1,3-dioxane was synthesized through the reaction of 2-(hydroxymethyl)-1,4-butanediol and 2,2-methoxy propane,the catalyst was added methyl-p-toluenesulfonate,2,2-methoxy propane dosage and the effect of the solvent on the yield.The results showed that the optimum reaction time of 10 h and the product yield of 72%.