2005Unpublished venueRequires access

Microwave Synthesis of α,α′-Bis(benzylidene) Cyclohexanone

Qing Tong

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Abstract

α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.

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What this paper is about

α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.

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Available abstract

α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.

Key concepts: Cyclohexanone, Formaldehyde, Yield (engineering), Catalysis, Fourier transform infrared spectroscopy, Chemistry, Proton NMR, Microwave

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