Microwave Synthesis of α,α′-Bis(benzylidene) Cyclohexanone
Qing Tong
Abstract
Qing Tong
Abstract
α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.
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α,α′-Bis(benzylidene) cyclohexanone was successfully prepared from phenyl formaldehyde and cyclohexanone at base conditions by the means of phase transfer catalysis method and microwave technology. The compound was characterized by FTIR、 1 HNMR and MS. This method had some advantages of simple operation, high yield and little contamination.
Key concepts: Cyclohexanone, Formaldehyde, Yield (engineering), Catalysis, Fourier transform infrared spectroscopy, Chemistry, Proton NMR, Microwave