2004Tianran chanwu yanjiu yu kaifaRequires access

STUDIES ON WATER-SOLUBLE CHEMICAL CONSTITUENTS OF RABDOSIA RUBESCENS

Weisheng Feng

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Abstract

Rabdosia rubescens(Hemls.) Hara was homogenized in an aqueous acetone.Five compounds were isolated over column chromatography on Diaion HP-20?Toyopearl HW-40?MCI Gel and silica gel.Aided with IR,MS and NMR spectra,their structures were identified as α-D-furanfructose(1),ferulic acid(2),n-butyl 3,4-dihydroxy-phenyl-lactate(3),3,4-dihydroxyphenyl-lactic acid(4),ent-7β,20-expoxykaur-16-ene-1α,6β,7β,14β,15β-pentaol-1-O-β-D-glucopy-ranoside(5).Compounds 1,2,3 and 4 were obtained from this plant and it's genus for the first time.

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What this paper is about

Rabdosia rubescens(Hemls.) Hara was homogenized in an aqueous acetone.Five compounds were isolated over column chromatography on Diaion HP-20?Toyopearl HW-40?MCI Gel and silica gel.Aided with IR,MS and NMR spectra,their structures were identified as α-D-furanfructose(1),ferulic acid(2),n-butyl 3,4-dihydroxy-phenyl-lactate(3),3,4-dihydroxyphenyl-lactic acid(4),ent-7β,20-expoxykaur-16-ene-1α,6β,7β,14β,15β-pentaol-1-O-β-D-glucopy-ranoside(5).Compounds 1,2,3 and 4 were obtained from this plant and it's genus for the first time.

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Available abstract

Rabdosia rubescens(Hemls.) Hara was homogenized in an aqueous acetone.Five compounds were isolated over column chromatography on Diaion HP-20?Toyopearl HW-40?MCI Gel and silica gel.Aided with IR,MS and NMR spectra,their structures were identified as α-D-furanfructose(1),ferulic acid(2),n-butyl 3,4-dihydroxy-phenyl-lactate(3),3,4-dihydroxyphenyl-lactic acid(4),ent-7β,20-expoxykaur-16-ene-1α,6β,7β,14β,15β-pentaol-1-O-β-D-glucopy-ranoside(5).Compounds 1,2,3 and 4 were obtained from this plant and it's genus for the first time.

Key concepts: Silica gel, Chemistry, Ferulic acid, Column chromatography, Chromatography, Acetone, Lactic acid, Organic chemistry

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