2011Tianran chanwu yanjiu yu kaifaRequires access

Chemical Constituents from Polygonum capitatum

Liu Ai-qin

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Abstract

Nine compounds were isolated from EtOAc extract of the Polygonum capitatum Buch.-Ham.ex D.Don..Their structures were identified as quercetin 3-O-(4″-O-acetyl)-α-L-rhamnopyranoside(1),quercetin(2),quercitrin(3),myricetrin(4),quercetin 3-rhamnoside 2″-gallate(5),protocatechuic acid(6),daucosterol(7),gallic acid(8) and progallin A(9) on the basis of their physical properties and the spectral data.Compound 1 was isolated from the genus Polygonum for the first time,and 4 was isolated from the plant for the first time.The NMR spectroscopic characteristics of the acetylated rhamnose of flavonoids glycosides were summarized.

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What this paper is about

Nine compounds were isolated from EtOAc extract of the Polygonum capitatum Buch.-Ham.ex D.Don..Their structures were identified as quercetin 3-O-(4″-O-acetyl)-α-L-rhamnopyranoside(1),quercetin(2),quercitrin(3),myricetrin(4),quercetin 3-rhamnoside 2″-gallate(5),protocatechuic acid(6),daucosterol(7),gallic acid(8) and progallin A(9) on the basis of their physical properties and the spectral data.Compound 1 was isolated from the genus Polygonum for the first time,and 4 was isolated from the plant for the first time.The NMR spectroscopic characteristics of the acetylated rhamnose of flavonoids glycosides were summarized.

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Available abstract

Nine compounds were isolated from EtOAc extract of the Polygonum capitatum Buch.-Ham.ex D.Don..Their structures were identified as quercetin 3-O-(4″-O-acetyl)-α-L-rhamnopyranoside(1),quercetin(2),quercitrin(3),myricetrin(4),quercetin 3-rhamnoside 2″-gallate(5),protocatechuic acid(6),daucosterol(7),gallic acid(8) and progallin A(9) on the basis of their physical properties and the spectral data.Compound 1 was isolated from the genus Polygonum for the first time,and 4 was isolated from the plant for the first time.The NMR spectroscopic characteristics of the acetylated rhamnose of flavonoids glycosides were summarized.

Key concepts: Quercitrin, Polygonum, Quercetin, Protocatechuic acid, Chemistry, Gallic acid, Daucosterol, Methyl gallate

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