ScholarLens Back to search
2007•Journal of Gansu SciencesRequires access

Solvent-Free Synthesis of Substituted Benzyl Benzoate under Microwave Irradiation Condition

Lin Bai

Open publisher page 0 citations

Abstract

The substituted benzyl benzoate was directly synthesized by benzyl chloride with substituted benzoic acid and K2CO3 under microwave irradiation and in presence of phase transfer catalyst without any solvent and inorganic carrier.TBAC solution has the best catalytic capability and the reaction was found to proceed well.When the microwave power was 375 W,the time of irradiation was 8 min,n(substituted benzoic acid)∶n(benzyl chloride)∶n(K2CO3)∶n(TBAC)=1∶2∶1∶0.075,the yield is up to 90%.

About this research paper

What this paper is about

The substituted benzyl benzoate was directly synthesized by benzyl chloride with substituted benzoic acid and K2CO3 under microwave irradiation and in presence of phase transfer catalyst without any solvent and inorganic carrier.TBAC solution has the best catalytic capability and the reaction was found to proceed well.When the microwave power was 375 W,the time of irradiation was 8 min,n(substituted benzoic acid)∶n(benzyl chloride)∶n(K2CO3)∶n(TBAC)=1∶2∶1∶0.075,the yield is up to 90%.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

The substituted benzyl benzoate was directly synthesized by benzyl chloride with substituted benzoic acid and K2CO3 under microwave irradiation and in presence of phase transfer catalyst without any solvent and inorganic carrier.TBAC solution has the best catalytic capability and the reaction was found to proceed well.When the microwave power was 375 W,the time of irradiation was 8 min,n(substituted benzoic acid)∶n(benzyl chloride)∶n(K2CO3)∶n(TBAC)=1∶2∶1∶0.075,the yield is up to 90%.

Key concepts: Benzoic acid, Catalysis, Microwave irradiation, Yield (engineering), Microwave, Chemistry, Solvent, Irradiation

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Solvent-Free Synthesis of Substituted Benzyl Benzoate under Microwave Irradiation Condition — Research Paper | ScholarLens