2003Unpublished venueRequires access

Catalytic Synthesis of Dibutyl Sebacate with Cupric Sulphfate

Deng Bin

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Abstract

Use of cupric sulphfate as catalyst on the esterification of dibutyl sebacate was studied The optimized conditions are as following:the weight of catalyst is 3 0g/0 05mol sebacic acid,the mole ratio of alchol to acid is 4,the reaction tim is 3 0h and 12ml benzene as water carrier The esterification yield for sebacic acid is about 97 23% Experimental results showed that cupric sulfate is a highly active catalyst for this reaction Less catalyst is required with little waste dischargement It is an inexpensive and very practical method

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Use of cupric sulphfate as catalyst on the esterification of dibutyl sebacate was studied The optimized conditions are as following:the weight of catalyst is 3 0g/0 05mol sebacic acid,the mole ratio of alchol to acid is 4,the reaction tim is 3 0h and 12ml benzene as water carrier The esterification yield for sebacic acid is about 97 23% Experimental results showed that cupric sulfate is a highly active catalyst for this reaction Less catalyst is required with little waste dischargement It is an inexpensive and very practical method

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Available abstract

Use of cupric sulphfate as catalyst on the esterification of dibutyl sebacate was studied The optimized conditions are as following:the weight of catalyst is 3 0g/0 05mol sebacic acid,the mole ratio of alchol to acid is 4,the reaction tim is 3 0h and 12ml benzene as water carrier The esterification yield for sebacic acid is about 97 23% Experimental results showed that cupric sulfate is a highly active catalyst for this reaction Less catalyst is required with little waste dischargement It is an inexpensive and very practical method

Key concepts: Sebacic acid, Catalysis, Yield (engineering), Benzene, Chemistry, Nuclear chemistry, Organic chemistry, Materials science

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