2007Wuji huaxue xuebaoRequires access

One-step Synthesis of ZnO Nanorods by Low-temperature Solution Method

Zhi Chen

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Abstract

By using ZnSO47H2O and NaOH as raw materials, C18H29NaO3S (DBS) as assistant, ZnO nanorods were synthesized directly in aqueous solution at low-temperature. TG-DSC, XRD, TEM and HRTEM results show that the crystal phase of the as-prepared ZnO nanorods has a hexagonal wurtzite structure with diameter from 30 to 50 nm and length up to 500 nm. The crystals grow along [001] direction. The mechanism for the ZnO nanorods growth was also discussed.

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What this paper is about

By using ZnSO47H2O and NaOH as raw materials, C18H29NaO3S (DBS) as assistant, ZnO nanorods were synthesized directly in aqueous solution at low-temperature. TG-DSC, XRD, TEM and HRTEM results show that the crystal phase of the as-prepared ZnO nanorods has a hexagonal wurtzite structure with diameter from 30 to 50 nm and length up to 500 nm. The crystals grow along [001] direction. The mechanism for the ZnO nanorods growth was also discussed.

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Available abstract

By using ZnSO47H2O and NaOH as raw materials, C18H29NaO3S (DBS) as assistant, ZnO nanorods were synthesized directly in aqueous solution at low-temperature. TG-DSC, XRD, TEM and HRTEM results show that the crystal phase of the as-prepared ZnO nanorods has a hexagonal wurtzite structure with diameter from 30 to 50 nm and length up to 500 nm. The crystals grow along [001] direction. The mechanism for the ZnO nanorods growth was also discussed.

Key concepts: Nanorod, Wurtzite crystal structure, High-resolution transmission electron microscopy, Materials science, Aqueous solution, Chemical engineering, Hexagonal crystal system, Phase (matter)

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