2006•Jilin Normal University JournalRequires access

Hydrothermal Synthesis and Crystal Structure of a New Supramolecular Compound[C_(10)H_9N_2][C_(10)H_(10)N_2][PW_(12)O_(40)]·2H_2O

Heng-Da Li

Abstract

A new supramolecular compound has been synthesized under hydrodthermal conditions and charac- terized by elemental analysis,IR and single-crystal X-ray diffraction.It shows that the compound crystallizes in the monoclinic system,space group C_2/m,a=1.2831(2)nm,b=2.052 1(3)nm,c=1.002 1(2)nm, V=2.3224(5)nm~3,Z=2,R_1=0.0529,WR_2=0.1428.

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Key concepts: Monoclinic crystal system, Supramolecular chemistry, Crystallography, Crystal structure, Hydrothermal synthesis, Chemistry, Hydrothermal reaction, Hydrothermal circulation