ScholarLens Back to search
2013•Physical Testing and Chemical AnalysisRequires access

ICP-AES Determination of 15 Impurity Elements in V-Al Alloy

Yong Cheng

Open publisher page 0 citations

Abstract

A method for the determination of 15 impurity elements including B,W,Si,Fe,Pb,Sn,As,Ni, Cr,Co,Cu,P,Mn,Mg and Mo,in V-Al alloy by ICP-AES was proposed.The spectral interferences were corrected by selection of analytical spectral lines and background correction positions;and matrix interferences were eliminated by the use of matrix-matching and synchronous background correctioa Values of detection limit(3s) of the method and of background equivalent concentration were found in ranges of 5.0-100μg·L~(-1) and 5 - 95μg·L~(-1) respectively.The proposed method was applied to the analysis of samples of V-Al alloys,and the results obtained were in consistency with those obtained by GfE Company.Values of recovery of the method were found in the range of 95.3%-110%,and values of RSD's(n = 8) were found5.0%(ω≥0.010%) and9.0%(ω= 0.001%～0.010%).

About this research paper

What this paper is about

A method for the determination of 15 impurity elements including B,W,Si,Fe,Pb,Sn,As,Ni, Cr,Co,Cu,P,Mn,Mg and Mo,in V-Al alloy by ICP-AES was proposed.The spectral interferences were corrected by selection of analytical spectral lines and background correction positions;and matrix interferences were eliminated by the use of matrix-matching and synchronous background correctioa Values of detection limit(3s) of the method and of background equivalent concentration were found in ranges of 5.0-100μg·L~(-1) and 5 - 95μg·L~(-1) respectively.The proposed method was applied to the analysis of samples of V-Al alloys,and the results obtained were in consistency with those obtained by GfE Company.Values of recovery of the method were found in the range of 95.3%-110%,and values of RSD's(n = 8) were found5.0%(ω≥0.010%) and9.0%(ω= 0.001%～0.010%).

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

A method for the determination of 15 impurity elements including B,W,Si,Fe,Pb,Sn,As,Ni, Cr,Co,Cu,P,Mn,Mg and Mo,in V-Al alloy by ICP-AES was proposed.The spectral interferences were corrected by selection of analytical spectral lines and background correction positions;and matrix interferences were eliminated by the use of matrix-matching and synchronous background correctioa Values of detection limit(3s) of the method and of background equivalent concentration were found in ranges of 5.0-100μg·L~(-1) and 5 - 95μg·L~(-1) respectively.The proposed method was applied to the analysis of samples of V-Al alloys,and the results obtained were in consistency with those obtained by GfE Company.Values of recovery of the method were found in the range of 95.3%-110%,and values of RSD's(n = 8) were found5.0%(ω≥0.010%) and9.0%(ω= 0.001%～0.010%).

Key concepts: Impurity, Alloy, Analytical Chemistry (journal), Detection limit, Matrix (chemical analysis), Inductively coupled plasma atomic emission spectroscopy, Materials science, Consistency (knowledge bases)

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
ICP-AES Determination of 15 Impurity Elements in V-Al Alloy — Research Paper | ScholarLens