Determination of Residual flubendiamide in Cabbage by HPLC
LI Mei-ling
Abstract
LI Mei-ling
Abstract
Using acetonitrile as extracting solvent,the residual flubendiamide in cabbage was extracted by ultrasonic extract method.Purified by QuEChERS,flubendiamide residue was analyzed by high performance liquid chromatography(HPLC) with UV detector.The results indicated that the average recoveries of flubendiamide in cabbage were 81.12%-89.61%,the variation coefficients were 1.51%-3.57% and the limit of quantification was 0.005 mg/kg.The technology could be used simply and efficiently for determination of flubendiamide residue.
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Using acetonitrile as extracting solvent,the residual flubendiamide in cabbage was extracted by ultrasonic extract method.Purified by QuEChERS,flubendiamide residue was analyzed by high performance liquid chromatography(HPLC) with UV detector.The results indicated that the average recoveries of flubendiamide in cabbage were 81.12%-89.61%,the variation coefficients were 1.51%-3.57% and the limit of quantification was 0.005 mg/kg.The technology could be used simply and efficiently for determination of flubendiamide residue.
Key concepts: Quechers, Chromatography, Residue (chemistry), High-performance liquid chromatography, Chemistry, Residual, Solvent, Acetonitrile