2006•Journal of Liaocheng UniversityRequires access

Synthesis and Crystal Structure of the [Cu(C_2H_8N_2)_2(H_2O)_2]_2[Fe(CN)_6]4H_2O

Dou Jian-min

Abstract

The title complex [Cu(C_2H_8N_2)_2(H_2O)_2]_2[Fe(CN)_6]4H_2O has been synthesized and characterized by elemental analysis,IR spectrum and X-ray diffraction analysis.The complex belongs to monoclinic,space group 2C/c ,with cell dimensions.a=0.794 7(4)nm,b=0.899 8(5)nm,c=1.095 4(6)nm,β=91.380(8)°,V=0.767 7(7)nm~3,Z=1,F(000)=378,R_1=0.039 9,wR_2=0.093 7.

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Key concepts: Monoclinic crystal system, Crystallography, Crystal structure, Chemistry, X-ray crystallography, Diffraction, Physics, Optics