Min Guo
Abstract
A high purity of ethoxyacetyl chloride was synthesized from ethoxyacetyl acid and thionyl chloride.Optimal reaction conditions were obtained based on orthogonal experiments that the molar ratio of thionyl chloride to ethoxyacetyl acid was 5 to 1,the catalyst was DMF and the reaction time was 16 h.
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A high purity of ethoxyacetyl chloride was synthesized from ethoxyacetyl acid and thionyl chloride.Optimal reaction conditions were obtained based on orthogonal experiments that the molar ratio of thionyl chloride to ethoxyacetyl acid was 5 to 1,the catalyst was DMF and the reaction time was 16 h.
Key concepts: Thionyl chloride, Chemistry, Molar ratio, Chloride, Catalysis, Nuclear chemistry, Organic chemistry, Inorganic chemistry