Zhi-Bin Cai
Abstract
m-Anisidine was synthesized from m-aminophenol by acetylation,methylation and alkali hydrolysis reaction in yield of 90.7%,82.8% and 88.2%,respectively.The optimum methylation reaction conditions were: m-hydroxyacetanilide 56 mmol,n(m-hydroxyacetanilide) ∶n(Me_2SO_4) ∶n(NaOH)=1.0 ∶1.5 ∶1.2,refluxing for 8 h,carbon tetrachloride as solvent.
A significance statement is not available in the OpenAlex record.
A contribution statement is not available in the OpenAlex record.
Method details are not available in the OpenAlex metadata.
Findings are not separately available in the OpenAlex metadata.
Limitations are not available in the OpenAlex metadata.
Application details are not available in the OpenAlex metadata.
m-Anisidine was synthesized from m-aminophenol by acetylation,methylation and alkali hydrolysis reaction in yield of 90.7%,82.8% and 88.2%,respectively.The optimum methylation reaction conditions were: m-hydroxyacetanilide 56 mmol,n(m-hydroxyacetanilide) ∶n(Me_2SO_4) ∶n(NaOH)=1.0 ∶1.5 ∶1.2,refluxing for 8 h,carbon tetrachloride as solvent.
Key concepts: Chemistry, Yield (engineering), Hydrolysis, Alkali metal, Solvent, Carbon tetrachloride, Nuclear chemistry, Acetylation