2011•Hunan Agricultural SciencesRequires access

Determination of Chromium in Vegetables by Microwave Digestion and Zeeman Graphite Furnace Atomic Absorption Spectrometry

Jingjing Yao

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Abstract

Using microwave digestion method to treat samples,and using Zeeman graphite furnace atomic absorption spectrometry(ZGFAAS) to determine chromium in vegetables.The results showed that when concentration of chromium was in a range of 0~25 μg/L,its linearity was great,correlation coefficient was larger than 0.999 5,recovery of standard addition was 96.2%~103.9%,RSD was 2.2%,and detection limit was 0.138 μg/L.This method has some advantages such as simple,rapid and accurate and reliable results.

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Using microwave digestion method to treat samples,and using Zeeman graphite furnace atomic absorption spectrometry(ZGFAAS) to determine chromium in vegetables.The results showed that when concentration of chromium was in a range of 0~25 μg/L,its linearity was great,correlation coefficient was larger than 0.999 5,recovery of standard addition was 96.2%~103.9%,RSD was 2.2%,and detection limit was 0.138 μg/L.This method has some advantages such as simple,rapid and accurate and reliable results.

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Available abstract

Using microwave digestion method to treat samples,and using Zeeman graphite furnace atomic absorption spectrometry(ZGFAAS) to determine chromium in vegetables.The results showed that when concentration of chromium was in a range of 0~25 μg/L,its linearity was great,correlation coefficient was larger than 0.999 5,recovery of standard addition was 96.2%~103.9%,RSD was 2.2%,and detection limit was 0.138 μg/L.This method has some advantages such as simple,rapid and accurate and reliable results.

Key concepts: Graphite furnace atomic absorption, Microwave digestion, Chromium, Zeeman effect, Detection limit, Atomic absorption spectroscopy, Analytical Chemistry (journal), Microwave

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