Determination Eugenol,Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography
Yang Dong-hua
Abstract
Yang Dong-hua
Abstract
Objective:The GC method was established for determination simulataneo of eugenol,borneol and isoborneol of Guanxin Shutong capsule.Method:The stationary phase of capillary column is polyethyleneglycol 20 000,with 10% coating.Carrier gas is nitrogen,detector is Flame Ionization Detector(FID).Result:The standard curve was linear within the concentration range of 2.025 6-50.640 0 μg(r=0.999 0) for eugenol,29.9-104.65 μg(r=0.999 5) for borneol.and 30.2-105.7 μg(r=0.999 4) for isoborneol The average recovery of eugenol,borneol and isoborneol was 100.95%(n=6,RSD 0.72%),99.72%(n=6,RSD 0.38%) and 100.47%(n=6,RSD 1.11%).Conclusion:The contents of eugenol,borneol and isoborneol in Guanxin Shutong capsule were determined in the first time.The method is simple,stability and feasible,controllable strong,which can beused to determinate the content of eugenol,borneol and isoborneol of Guanxin Shutong capsule.
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Objective:The GC method was established for determination simulataneo of eugenol,borneol and isoborneol of Guanxin Shutong capsule.Method:The stationary phase of capillary column is polyethyleneglycol 20 000,with 10% coating.Carrier gas is nitrogen,detector is Flame Ionization Detector(FID).Result:The standard curve was linear within the concentration range of 2.025 6-50.640 0 μg(r=0.999 0) for eugenol,29.9-104.65 μg(r=0.999 5) for borneol.and 30.2-105.7 μg(r=0.999 4) for isoborneol The average recovery of eugenol,borneol and isoborneol was 100.95%(n=6,RSD 0.72%),99.72%(n=6,RSD 0.38%) and 100.47%(n=6,RSD 1.11%).Conclusion:The contents of eugenol,borneol and isoborneol in Guanxin Shutong capsule were determined in the first time.The method is simple,stability and feasible,controllable strong,which can beused to determinate the content of eugenol,borneol and isoborneol of Guanxin Shutong capsule.
Key concepts: Borneol, Eugenol, Chromatography, Capsule, Chemistry, Gas chromatography, Analytical Chemistry (journal), Medicine