2011Physical Testing and Chemical AnalysisRequires access

Effect of Different Methods of Sample Digestion on the FAAS Determination of Inoganic Elements in Dairy Products

Rui Wang

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Abstract

Samples of fresh milk and yoghurt were pre-treated separately by 3 different methods of sample digestion,i.e.,the conventional wet acid digestion,the microwave assisted acid digestion and the dry ashing method,and the final sample solutions were used for FAAS determination of 6 inorganic elements,i.e.,Ca,Mg, Cu,Zn,Fe and Mn.As shown by the analytical results,the highest recovery of 94.5%—100.0%was obtained by the microwave assisted sample digestion method and values of RSD s(n = 6) obtained were in the range of 1.9%—4.2%.Hence,the microwave assisted digestion of samples of dairy products was preferred rather than the other 2 methods.

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What this paper is about

Samples of fresh milk and yoghurt were pre-treated separately by 3 different methods of sample digestion,i.e.,the conventional wet acid digestion,the microwave assisted acid digestion and the dry ashing method,and the final sample solutions were used for FAAS determination of 6 inorganic elements,i.e.,Ca,Mg, Cu,Zn,Fe and Mn.As shown by the analytical results,the highest recovery of 94.5%—100.0%was obtained by the microwave assisted sample digestion method and values of RSD s(n = 6) obtained were in the range of 1.9%—4.2%.Hence,the microwave assisted digestion of samples of dairy products was preferred rather than the other 2 methods.

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Available abstract

Samples of fresh milk and yoghurt were pre-treated separately by 3 different methods of sample digestion,i.e.,the conventional wet acid digestion,the microwave assisted acid digestion and the dry ashing method,and the final sample solutions were used for FAAS determination of 6 inorganic elements,i.e.,Ca,Mg, Cu,Zn,Fe and Mn.As shown by the analytical results,the highest recovery of 94.5%—100.0%was obtained by the microwave assisted sample digestion method and values of RSD s(n = 6) obtained were in the range of 1.9%—4.2%.Hence,the microwave assisted digestion of samples of dairy products was preferred rather than the other 2 methods.

Key concepts: Ashing, Digestion (alchemy), Chemistry, Chromatography, Microwave digestion, Sample preparation, Analytical Chemistry (journal), Detection limit

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