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Synthesis of 2,5-Bis(methoxycarbonyl)terephthaloyl Chloride and Fast Determination of Chlorine

Miaoqing Liu

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Abstract

Taking pyromellitic dianhydride and thionyl chloride as raw key material, 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized. Chlorine determination method was introduced to indicate its purity. The melting point equipment, IR and 1H NMR techniques were used to characterize the product. The results showed that the purity of 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized.

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What this paper is about

Taking pyromellitic dianhydride and thionyl chloride as raw key material, 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized. Chlorine determination method was introduced to indicate its purity. The melting point equipment, IR and 1H NMR techniques were used to characterize the product. The results showed that the purity of 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized.

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Available abstract

Taking pyromellitic dianhydride and thionyl chloride as raw key material, 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized. Chlorine determination method was introduced to indicate its purity. The melting point equipment, IR and 1H NMR techniques were used to characterize the product. The results showed that the purity of 2,5-bis(methoxycarbonyl)terephthaloyl chloride was synthesized.

Key concepts: Terephthaloyl chloride, Thionyl chloride, Chlorine, Chemistry, Chloride, Melting point, Raw material, Polymer chemistry

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