2000Journal of Gansu Education CollegeRequires access

Catalytic Synthesis of Dibutyl Phthalate by P-Toluene Sulphonic Acid

Shuyun Liu

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Abstract

Dibutyl phthalate was sy nthesized from phthalic anhydride and n-butyl alcohol in presence of p-toluene sulphonic acid. The yield of the ester could reach 98% when the mole ratio of p hthalic anhydride ,n-butyl alcohol and p-toluene sulphonic acid was 1∶4∶0. 05,with refluxing and segrating water for 3.0 h.

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What this paper is about

Dibutyl phthalate was sy nthesized from phthalic anhydride and n-butyl alcohol in presence of p-toluene sulphonic acid. The yield of the ester could reach 98% when the mole ratio of p hthalic anhydride ,n-butyl alcohol and p-toluene sulphonic acid was 1∶4∶0. 05,with refluxing and segrating water for 3.0 h.

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Available abstract

Dibutyl phthalate was sy nthesized from phthalic anhydride and n-butyl alcohol in presence of p-toluene sulphonic acid. The yield of the ester could reach 98% when the mole ratio of p hthalic anhydride ,n-butyl alcohol and p-toluene sulphonic acid was 1∶4∶0. 05,with refluxing and segrating water for 3.0 h.

Key concepts: Dibutyl phthalate, Phthalic anhydride, Toluene, Chemistry, Alcohol, Catalysis, Organic chemistry, Phthalic acid

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