Catalytic synthesis of dibutyl adipate with p - toluene sulphonic acid
Shan Li
Abstract
Shan Li
Abstract
Dibutyl adipate was synthesis from adipic acid and n - butyl alcohol in the presence of p - toluene sulphonic acid. The yield of the ester could reach 96.9% under amount of substance ratio of adipic acid, n - butyl alcohol and p - toluene sulphonic acid were 1 :4:0.2, refluxing and water segrating for 30min.
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Dibutyl adipate was synthesis from adipic acid and n - butyl alcohol in the presence of p - toluene sulphonic acid. The yield of the ester could reach 96.9% under amount of substance ratio of adipic acid, n - butyl alcohol and p - toluene sulphonic acid were 1 :4:0.2, refluxing and water segrating for 30min.
Key concepts: Adipic acid, Toluene, Adipate, Chemistry, Alcohol, Catalysis, Yield (engineering), Organic chemistry