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Determination of Ba content in Si-Al-Ba Alloys by ICP-AES

Zhaohua Song

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Abstract

A method of determining the Ba content in Si-Al-Ba Alloys by ICP-AES was developed, in which the alloy was dissolved in a mixed acid of HF-HNO_3-HClO_4, and the Ba content was determined using the 233.527 nm peak of Ba. Being simple, quick, precise and accurate in operation, this method has yielded a recovery rate of 99%~100% with samples containing calibrating additions, and in a relative standard deviations of 0.25%~0.56%.

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A method of determining the Ba content in Si-Al-Ba Alloys by ICP-AES was developed, in which the alloy was dissolved in a mixed acid of HF-HNO_3-HClO_4, and the Ba content was determined using the 233.527 nm peak of Ba. Being simple, quick, precise and accurate in operation, this method has yielded a recovery rate of 99%~100% with samples containing calibrating additions, and in a relative standard deviations of 0.25%~0.56%.

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Available abstract

A method of determining the Ba content in Si-Al-Ba Alloys by ICP-AES was developed, in which the alloy was dissolved in a mixed acid of HF-HNO_3-HClO_4, and the Ba content was determined using the 233.527 nm peak of Ba. Being simple, quick, precise and accurate in operation, this method has yielded a recovery rate of 99%~100% with samples containing calibrating additions, and in a relative standard deviations of 0.25%~0.56%.

Key concepts: Inductively coupled plasma atomic emission spectroscopy, Relative standard deviation, Alloy, Content (measure theory), Analytical Chemistry (journal), Recovery rate, Materials science, Inductively coupled plasma

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