Determinating Calcium and Alumintum and Barium in Alloy with ICP-AES
Shiqin Jiang
Abstract
Shiqin Jiang
Abstract
Through method of measuring Calcium,Barium,and Aluminum in Si-Al-Ba-Ca by ICP-AES,the best measuring conditions were established.The influence of acid and alkali for dissolution and coexisting ions in sample were studied,and accuracy and precision of the experiment were measured.The relative standard deviation(%) was Ca 0.33,Ba 0.52,and A 0.32.The relative error of determined value was-0.31%~0.50%.It was proved the method was simple and fast,which realized simulaneous online analysis of Ca,Ba,and Al and can be used in the production analysis.
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Through method of measuring Calcium,Barium,and Aluminum in Si-Al-Ba-Ca by ICP-AES,the best measuring conditions were established.The influence of acid and alkali for dissolution and coexisting ions in sample were studied,and accuracy and precision of the experiment were measured.The relative standard deviation(%) was Ca 0.33,Ba 0.52,and A 0.32.The relative error of determined value was-0.31%~0.50%.It was proved the method was simple and fast,which realized simulaneous online analysis of Ca,Ba,and Al and can be used in the production analysis.
Key concepts: Barium, Inductively coupled plasma atomic emission spectroscopy, Analytical Chemistry (journal), Calcium, Alkali metal, Dissolution, Relative standard deviation, Materials science