2010Fine and Specialty ChemicalsRequires access

Catalytic synthesis of butanone 1,2-propanediol ketal with cerium sulfate

Yang Shui-jin

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Abstract

Butanone 1,2-propanediol ketal was synthesized from butanone and 1,2-propanediol using cerium sulfate as catalyst.The factors influencing the synthesis were investigated.The optimum conditions were as follows: n(butanone):n(l,2-propanediol) is 1:1.5,w(catalyst) is 1.6%,and the reaction time is 75min.Cerium sulfate is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal and the product yield can reach over 82.7%.

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What this paper is about

Butanone 1,2-propanediol ketal was synthesized from butanone and 1,2-propanediol using cerium sulfate as catalyst.The factors influencing the synthesis were investigated.The optimum conditions were as follows: n(butanone):n(l,2-propanediol) is 1:1.5,w(catalyst) is 1.6%,and the reaction time is 75min.Cerium sulfate is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal and the product yield can reach over 82.7%.

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Available abstract

Butanone 1,2-propanediol ketal was synthesized from butanone and 1,2-propanediol using cerium sulfate as catalyst.The factors influencing the synthesis were investigated.The optimum conditions were as follows: n(butanone):n(l,2-propanediol) is 1:1.5,w(catalyst) is 1.6%,and the reaction time is 75min.Cerium sulfate is an excellent catalyst for synthesizing butanone 1,2-propanediol ketal and the product yield can reach over 82.7%.

Key concepts: Butanone, Catalysis, Propanediol, Cerium, Yield (engineering), Chemistry, Sulfate, Organic chemistry

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