ScholarLens Back to search
2004•Analytical LaboratoryRequires access

Determination of caprolactam by flow-injection chemiluminescence analysis

Maotian Xu, Yaodong Liang

Open publisher page 0 citations

Abstract

A novel flow injection chemiluminescence (CL) system for caprolactam determination was proposed. It was based on that CL signal of Ce(Ⅳ)-SO_3~(2-) was strongly enhanced in the presence of caprolactam. The system showed a linear range of 4.0×10~(-7)～1.0×10~(-5) (g/mL) for caprolactam. The relative standard deviation (n=11) was 2.1% for 4.0×10~(-7) (g/mL) caprolactam and the detection limit was 1×10~(-7) (g/mL). The method was applied to the determination of caprolactam in polycaprolactam samples with satisfactory results.

About this research paper

What this paper is about

A novel flow injection chemiluminescence (CL) system for caprolactam determination was proposed. It was based on that CL signal of Ce(Ⅳ)-SO_3~(2-) was strongly enhanced in the presence of caprolactam. The system showed a linear range of 4.0×10~(-7)～1.0×10~(-5) (g/mL) for caprolactam. The relative standard deviation (n=11) was 2.1% for 4.0×10~(-7) (g/mL) caprolactam and the detection limit was 1×10~(-7) (g/mL). The method was applied to the determination of caprolactam in polycaprolactam samples with satisfactory results.

Why it matters

A significance statement is not available in the OpenAlex record.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

A novel flow injection chemiluminescence (CL) system for caprolactam determination was proposed. It was based on that CL signal of Ce(Ⅳ)-SO_3~(2-) was strongly enhanced in the presence of caprolactam. The system showed a linear range of 4.0×10~(-7)～1.0×10~(-5) (g/mL) for caprolactam. The relative standard deviation (n=11) was 2.1% for 4.0×10~(-7) (g/mL) caprolactam and the detection limit was 1×10~(-7) (g/mL). The method was applied to the determination of caprolactam in polycaprolactam samples with satisfactory results.

Key concepts: Caprolactam, Chemiluminescence, Chemistry, Detection limit, Relative standard deviation, Linear range, Chromatography, Flow injection analysis

Related papers

Related paper 1Related paper 2Related paper 3
Back to paper searchBrowse research topicsOriginal source
Determination of caprolactam by flow-injection chemiluminescence analysis — Research Paper | ScholarLens