Synthesis of 2,3,5,6-Tetrabenzylpyrazine under Microwave Irradiation
Hongya Li
Abstract
Hongya Li
Abstract
2,3,5,6-Tetrabenzylpyrazine(2) in yield of 51% was synthesized by condensation of benzoin with AcONH4 in presence of Ac2O.The yield of 2 reached 68% under microwave irradiation for 6 min~10 min.The structure was characterized by 1H NMR and IR.
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2,3,5,6-Tetrabenzylpyrazine(2) in yield of 51% was synthesized by condensation of benzoin with AcONH4 in presence of Ac2O.The yield of 2 reached 68% under microwave irradiation for 6 min~10 min.The structure was characterized by 1H NMR and IR.
Key concepts: Chemistry, Yield (engineering), Microwave irradiation, Benzoin, Condensation, Nuclear chemistry, Irradiation, Proton NMR