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Synthesis of 1-Bromododecane Using Hydrobromic Acid Method

Heng Jiang

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Abstract

1-Bromododecane was synthesized from n-dodecyl alcohol using byproduct hydrobromic acid from 1-bromoadamantan process as raw material in the presence of the concentrated sulfuric acid.The optimal conditions were as follow:the molar ratio of n-dodecyl alcohol,hydrobromic acid and concentrated sulfuric acid was 1:1.25:1.15,the reaction time was 3 h.No by-product was detected in the product by GC.The yield of 1-bromododecane was 92.5%,and the purity was 99.9%.The product was characterized by IR and index of refraction.

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What this paper is about

1-Bromododecane was synthesized from n-dodecyl alcohol using byproduct hydrobromic acid from 1-bromoadamantan process as raw material in the presence of the concentrated sulfuric acid.The optimal conditions were as follow:the molar ratio of n-dodecyl alcohol,hydrobromic acid and concentrated sulfuric acid was 1:1.25:1.15,the reaction time was 3 h.No by-product was detected in the product by GC.The yield of 1-bromododecane was 92.5%,and the purity was 99.9%.The product was characterized by IR and index of refraction.

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Available abstract

1-Bromododecane was synthesized from n-dodecyl alcohol using byproduct hydrobromic acid from 1-bromoadamantan process as raw material in the presence of the concentrated sulfuric acid.The optimal conditions were as follow:the molar ratio of n-dodecyl alcohol,hydrobromic acid and concentrated sulfuric acid was 1:1.25:1.15,the reaction time was 3 h.No by-product was detected in the product by GC.The yield of 1-bromododecane was 92.5%,and the purity was 99.9%.The product was characterized by IR and index of refraction.

Key concepts: Hydrobromic acid, Chemistry, Sulfuric acid, Yield (engineering), Molar ratio, Alcohol, Raw material, Nuclear chemistry

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