2008Science & Technology in Chemical IndustryRequires access

Synthesis of 2-butyl bromide using hydrobromic acid method

Hong Gong

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Abstract

2-Butyl bromide was synthesized from hydrobromic acid(48%) and 2-butylalcohol by adding concentrated sulfuric acid.Various affecting factors were investigated.The result showed that the optimal conditions were 2-butylalcohol 0.16mol,hydrobromic acid 0.18mol,concentrated sulfuric acid 18mL,refluxed for 1h.The separated yield was high up to 95.00%.This method not only saves raw materials,but also has less pollution.

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What this paper is about

2-Butyl bromide was synthesized from hydrobromic acid(48%) and 2-butylalcohol by adding concentrated sulfuric acid.Various affecting factors were investigated.The result showed that the optimal conditions were 2-butylalcohol 0.16mol,hydrobromic acid 0.18mol,concentrated sulfuric acid 18mL,refluxed for 1h.The separated yield was high up to 95.00%.This method not only saves raw materials,but also has less pollution.

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Available abstract

2-Butyl bromide was synthesized from hydrobromic acid(48%) and 2-butylalcohol by adding concentrated sulfuric acid.Various affecting factors were investigated.The result showed that the optimal conditions were 2-butylalcohol 0.16mol,hydrobromic acid 0.18mol,concentrated sulfuric acid 18mL,refluxed for 1h.The separated yield was high up to 95.00%.This method not only saves raw materials,but also has less pollution.

Key concepts: Hydrobromic acid, Sulfuric acid, Chemistry, Bromide, Yield (engineering), Bromine, Raw material, Nuclear chemistry

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