Electroreduction of Oxalic Acid to Glycolic Acid
Yu Li
Abstract
Yu Li
Abstract
Electroreduction of oxalic acid to glycolic acid was confirmed by cyclic voltammetry.Glycolic acid was prepared from oxalic acid at the Pb cathode in an eletrolytic cell with cationexchange mambrane.By orthogonal experiments the optimal operating conditions were obtained:current density 1400 A/m2,electric quantity 17 F/mol,temperature 40 ℃ and flowrate of electrolyte 015 m/s?The yield was over 88%.
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Electroreduction of oxalic acid to glycolic acid was confirmed by cyclic voltammetry.Glycolic acid was prepared from oxalic acid at the Pb cathode in an eletrolytic cell with cationexchange mambrane.By orthogonal experiments the optimal operating conditions were obtained:current density 1400 A/m2,electric quantity 17 F/mol,temperature 40 ℃ and flowrate of electrolyte 015 m/s?The yield was over 88%.
Key concepts: Glycolic acid, Oxalic acid, Cyclic voltammetry, Chemistry, Electrolyte, Yield (engineering), Inorganic chemistry, Nuclear chemistry