2006•Rengong jingti xuebaoRequires access

Synthesis,Crystal Structure and Spectral Characterization of the Complex [Zn(CH_3COO)_2(C_7H_6N_2S)_2]

Weixing Ma, Bao‐Hua Qian, Qingfang Cheng, Xing-You Xu, Lude Lu

Abstract

A mixed complex [Zn(CH_(3)COO)_2(C_(7)H_(6)N_2S)_2]was synthesized based on the reaction of Zn(CH_(3)COO)_2and 2-aminobenzothiazol(C_(7)H_(6)N_2S)in methanol.The structure of the mixed complex was characterized by elemental analysis,IR,~1 H NMR and thermal analysis.The crystal structure of the complex was also determined by X-ray single crystal diffraction.The results show that the crystal belongs to orthorhombic system with space group Pna2(1),a=0.8547(3)nm,b=2.7586(8)nm,c=0.9066(3)nm,α=β=γ=90°,V=2.1376(11)nm~3;D_c=1.503g/cm~3;Z=4;F(000)=992;μ=1.375mm~(-1).

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Key concepts: Orthorhombic crystal system, Crystal structure, Crystallography, Materials science, Crystal (programming language), Methanol, Elemental analysis, Diffraction