Studies on chemical constituents of the total flavonoids from Comptosorus sibiricus Rupr.(1)
Nan Wang
Abstract
Nan Wang
Abstract
Objective To study the chemical constituents of the total flavonoids from the ethanol(ω=0.7)extract of the whole herb of Comptosorus sibiricus Rupr..Methods The compounds were isolated by chromatography on the silica gel column and identified on the basis of physico-chemical constants and spectral analysis.Result Six compounds were isolated as kaempferol(Ⅰ), kaempferol-7-O-α-L-rhamnoside(Ⅱ), kaempferol 3-O-β-D- glucopyranoside(Ⅲ),kaempferol 7-O-β-D-glucopyranoside(Ⅳ),kaempferol 3,7-di-O-β-D-glucopyranoside(Ⅴ),kaempferol-3-O-β-D- glucopyranoside -7-O-α-L-rhamnoside(Ⅵ)respectively.Conclusion Compound Ⅱ is obtained from this plant for the first time.
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Objective To study the chemical constituents of the total flavonoids from the ethanol(ω=0.7)extract of the whole herb of Comptosorus sibiricus Rupr..Methods The compounds were isolated by chromatography on the silica gel column and identified on the basis of physico-chemical constants and spectral analysis.Result Six compounds were isolated as kaempferol(Ⅰ), kaempferol-7-O-α-L-rhamnoside(Ⅱ), kaempferol 3-O-β-D- glucopyranoside(Ⅲ),kaempferol 7-O-β-D-glucopyranoside(Ⅳ),kaempferol 3,7-di-O-β-D-glucopyranoside(Ⅴ),kaempferol-3-O-β-D- glucopyranoside -7-O-α-L-rhamnoside(Ⅵ)respectively.Conclusion Compound Ⅱ is obtained from this plant for the first time.
Key concepts: Kaempferol, Chemistry, Silica gel, Chemical constituents, Column chromatography, Flavonoid, Chromatography, Stereochemistry