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Synthesis of Benzyl Benzoate under Microwave Irradiation and Phase Transfer Catalyst

Xiaoping Zhu

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Abstract

Benzyl Benzoate was directly synthesized from benzyl chloride and sodium benzoate under the condition of microwave irradiation and phase transfer catalyst without any organic solvent and inorganic carrier. The optimum conditions was as follow the microwave power 350W, the irradiation time 3min, TBAB as the phase transfer catalyst, the mole ratio of sodium benzoate to benzyl chloride 1.0∶1.6 and sodium benzoate to TBAB 25.0∶1.3, the yield is up to 98.9%.

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What this paper is about

Benzyl Benzoate was directly synthesized from benzyl chloride and sodium benzoate under the condition of microwave irradiation and phase transfer catalyst without any organic solvent and inorganic carrier. The optimum conditions was as follow the microwave power 350W, the irradiation time 3min, TBAB as the phase transfer catalyst, the mole ratio of sodium benzoate to benzyl chloride 1.0∶1.6 and sodium benzoate to TBAB 25.0∶1.3, the yield is up to 98.9%.

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Available abstract

Benzyl Benzoate was directly synthesized from benzyl chloride and sodium benzoate under the condition of microwave irradiation and phase transfer catalyst without any organic solvent and inorganic carrier. The optimum conditions was as follow the microwave power 350W, the irradiation time 3min, TBAB as the phase transfer catalyst, the mole ratio of sodium benzoate to benzyl chloride 1.0∶1.6 and sodium benzoate to TBAB 25.0∶1.3, the yield is up to 98.9%.

Key concepts: Chemistry, Sodium benzoate, Catalysis, Benzyl benzoate, Yield (engineering), Phase-transfer catalyst, Microwave, Phase (matter)

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