2004•Applied science and technologyRequires access
Synthesis of ethyl chloroacetate under the condition of microwave catalysis
Haiyang Wang
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Abstract
Under the condition of microwave, Ethyl chloroacetate can be synthetized by using strong H_2SO_4 as catalyst and chloroacetatic acid ethyl alcohol as reactants. The best reaction conditions are as follows: the mole ratio of chloroacetatic acid ethyl alcohol is 1:1.2; the amount of catalyst is 1.0 g; radiating time is 6 min;the power of the microwave is 230 W and the ratio of transforming is 73.8%.