2009•Chemical ResearchRequires access

Hydrothermal Synthesis and Structure of [Cu(en)_2]_2[Cu(en)_2(H_2O)][PW_(11.5)Cu_(0.5)O_(40)]·OH·3H_2O

MA Peng-tao

Abstract

A 1D chain compound based on Keggin anion [Cu(en)2]2[Cu(en)2(H2O)][PW11.5Cu0.5O40]·OH·3H2O was hydrothermally synthesized and characterized by IR,UV spectrometry and X-ray single-crystal diffraction.The title compound crystallizes in monoclinic system,P21/c space group,cell parameter: a=1.266 25(10),b=2.145 45(19),c=2.455 95(18) nm,β=114.919(3),V=6.050 9(8) nm3,Z=4,R1=0.068 1,wR2=0.146 8.

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Key concepts: Monoclinic crystal system, Crystallography, Hydrothermal circulation, Chemistry, Hydrothermal synthesis, Single crystal, Crystal structure, Copper