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1981•Bulletin of the Chemical Society of JapanRequires access

Synthesis and Reactions of Perylenecarboxylic Acid Derivatives. VII. Hydrolysis of N,N′-Dialkyl-3,4 : 9,10-Perylenebis(dicarboximide) with Sulfuric Acid

Yukinori Nagao, Takahisa MISONO

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Abstract

Abstract The hydrolysis of N,N′-dialkyl-3,4 : 9,10-perylenebis(dicarboximide) (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3) with sulfuric acid at 180–200 °C gave N-alkyl-3,4 : 9,10-perylenetetracarboxylic monoanhydride monoimide (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3). The kinetics of the reaction were determined spectroscopically.

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Abstract The hydrolysis of N,N′-dialkyl-3,4 : 9,10-perylenebis(dicarboximide) (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3) with sulfuric acid at 180–200 °C gave N-alkyl-3,4 : 9,10-perylenetetracarboxylic monoanhydride monoimide (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3). The kinetics of the reaction were determined spectroscopically.

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Available abstract

Abstract The hydrolysis of N,N′-dialkyl-3,4 : 9,10-perylenebis(dicarboximide) (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3) with sulfuric acid at 180–200 °C gave N-alkyl-3,4 : 9,10-perylenetetracarboxylic monoanhydride monoimide (alkyl=CH3, CH2CH3, CH2CH2CH3, and CH2CH2CH2CH3). The kinetics of the reaction were determined spectroscopically.

Key concepts: Chemistry, Sulfuric acid, Hydrolysis, Acid hydrolysis, Organic chemistry, Acid catalysis, Medicinal chemistry, Catalysis

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Synthesis and Reactions of Perylenecarboxylic Acid Derivatives. VII. Hydrolysis of N,N′-Dialkyl-3,4 : 9,10-Perylenebis(dicarboximide) with Sulfuric Acid — Research Paper | ScholarLens