2009•Journal of the Ceramic Society of JapanOpen access

Effect of AlN additive on densification, microstructure and strength of liquid-phase sintered SiC ceramics by spark plasma sintering

Mikinori Hotta, Junichi Hojo

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Abstract

SiC ceramics were prepared from β-SiC starting powder with AlN and Y2O3 sintering additives by spark plasma sintering. Densification, microstructure and flexural strength of the liquid-phase sintered SiC ceramics were investigated. The relative density of SiC sintered bodies reached over 95% at total amount of 10 vol% AlN and Y2O3 additives and at 1900°C for 600 s in N2 at 30 MPa. When the content of AlN additive increased, the size of SiC grains decreased. The SiC body almost without the grain growth was successfully prepared using 95 mol% AlN and 5 mol% Y2O3 additives. The flexural strength of the SiC body was 1150 MPa.

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SiC ceramics were prepared from β-SiC starting powder with AlN and Y2O3 sintering additives by spark plasma sintering. Densification, microstructure and flexural strength of the liquid-phase sintered SiC ceramics were investigated. The relative density of SiC sintered bodies reached over 95% at total amount of 10 vol% AlN and Y2O3 additives and at 1900°C for 600 s in N2 at 30 MPa. When the content of AlN additive increased, the size of SiC grains decreased. The SiC body almost without the grain growth was successfully prepared using 95 mol% AlN and 5 mol% Y2O3 additives. The flexural strength of the SiC body was 1150 MPa.

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Available abstract

SiC ceramics were prepared from β-SiC starting powder with AlN and Y2O3 sintering additives by spark plasma sintering. Densification, microstructure and flexural strength of the liquid-phase sintered SiC ceramics were investigated. The relative density of SiC sintered bodies reached over 95% at total amount of 10 vol% AlN and Y2O3 additives and at 1900°C for 600 s in N2 at 30 MPa. When the content of AlN additive increased, the size of SiC grains decreased. The SiC body almost without the grain growth was successfully prepared using 95 mol% AlN and 5 mol% Y2O3 additives. The flexural strength of the SiC body was 1150 MPa.

Key concepts: Materials science, Spark plasma sintering, Microstructure, Flexural strength, Sintering, Ceramic, Relative density, Phase (matter)

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Effect of AlN additive on densification, microstructure and strength of liquid-phase sintered SiC ceramics by spark plasma sintering — Research Paper | ScholarLens