2006•Journal of Separation ScienceRequires access

Monolithic enantiomer‐selective stationary phases for capillary electrochromatography

Feng Qin, Chuanhui Xie, Zhiyuan Yu, Liang Kong, Mingliang Ye, Hanfa Zou

Abstract

Monolithic materials have become a well-established format for stationary phases in the field of capillary electrochromatography. Four types of monoliths, namely particle-fixed, silica-based, polymer-based, and molecularly imprinted monoliths, have been utilized as enantiomer-selective stationary phases in CEC. This review summarizes recent developments in the area of monolithic enantiomer-selective stationary phases for CEC. The preparative procedure and the characterization of these columns are highlighted. In addition, the disadvantages and limitations of different monolithic enantiomer-selective stationary phases in CEC are briefly discussed.

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Key concepts: Capillary electrochromatography, Enantiomer, Electrochromatography, Chiral stationary phase, Monolithic HPLC column, Chemistry, Capillary electrophoresis, Stationary phase