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2013•Journal of Physics Conference SeriesOpen access

SAXS/WAXS Capability and Absolute Intensity Measurement Study at the SAXS Beamline of the Siam Photon Laboratory

Rarm Phinjaroenphan, Siriwat Soontaranon, Prae Chirawatkul, Jitrin Chaiprapa, Wutthikrai Busayaporn, Surachai Pongampai, Supanan Lapboonreung, Supagorn Rugmai

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Abstract

A Small Angle X-ray Scattering (SAXS) beamline has been constructed at the Siam Photon Laboratory of the Synchrotron Light Research Institute (SLRI), Thailand. The beamline was commissioned and opened for users in March 2011. In order to maximize the photon flux, a Double Multilayer Monochromator was adopted to monochromatize synchrotron x-rays within the energy range of 6-9 keV. The experimental station is equipped with a CCD detector for SAXS measurements and an Image Plate for wide angle x-ray scattering (WAXS) measurements. Apparatus for in-situ measurements have been developed to enable studies of nano structural changes during temperature and tensile variation. Capability for scattering measurements in absolute unit has been investigated. This work reports the current status of the beamline and results from dispersed Au nanoparticles measurements.

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A Small Angle X-ray Scattering (SAXS) beamline has been constructed at the Siam Photon Laboratory of the Synchrotron Light Research Institute (SLRI), Thailand. The beamline was commissioned and opened for users in March 2011. In order to maximize the photon flux, a Double Multilayer Monochromator was adopted to monochromatize synchrotron x-rays within the energy range of 6-9 keV. The experimental station is equipped with a CCD detector for SAXS measurements and an Image Plate for wide angle x-ray scattering (WAXS) measurements. Apparatus for in-situ measurements have been developed to enable studies of nano structural changes during temperature and tensile variation. Capability for scattering measurements in absolute unit has been investigated. This work reports the current status of the beamline and results from dispersed Au nanoparticles measurements.

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Available abstract

A Small Angle X-ray Scattering (SAXS) beamline has been constructed at the Siam Photon Laboratory of the Synchrotron Light Research Institute (SLRI), Thailand. The beamline was commissioned and opened for users in March 2011. In order to maximize the photon flux, a Double Multilayer Monochromator was adopted to monochromatize synchrotron x-rays within the energy range of 6-9 keV. The experimental station is equipped with a CCD detector for SAXS measurements and an Image Plate for wide angle x-ray scattering (WAXS) measurements. Apparatus for in-situ measurements have been developed to enable studies of nano structural changes during temperature and tensile variation. Capability for scattering measurements in absolute unit has been investigated. This work reports the current status of the beamline and results from dispersed Au nanoparticles measurements.

Key concepts: Beamline, Small-angle X-ray scattering, Monochromator, Synchrotron, Scattering, Materials science, Optics, Synchrotron radiation

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SAXS/WAXS Capability and Absolute Intensity Measurement Study at the SAXS Beamline of the Siam Photon Laboratory — Research Paper | ScholarLens