1979Journal of Vacuum Science and TechnologyRequires access

Cryogenic pumping of helium, hydrogen, and a 90% hydrogen–10% helium mixture

C. F. Dillow, J.M. Palacios

Open publisher page 7 citations

Abstract

An experimental program to measure the pumping speed of an Excalibur CVV2008 liquid helium cryosorption pump is described. Pumping speeds are reported for helium, hydrogen, and a 90% hydrogen –10% helium mixture in the pressure range 1×10−7–1×10−4 Torr. The helium pumping speed at 2×10−7 Torr was 3.2 l/s cm2, but decreased with loading to 1.6 l/s cm2 at 6×10−5 Torr. Attempts to operate at higher helium fluxes (Q≳8×10−5 sccm/s cm2) resulted in pressure and eventually thermal instabilities. The pumping speed of hydrogen at 5×10−7 Torr was 4.9 l/s cm2 and increased with pressure to 7.7 l/s cm2 at 5.5×10−6 Torr. For a 90% hydrogen–10% helium mixture, pumping speeds were inconsistent, varying between 1.4 and 5.6 l/s cm2. Residual gas analysis provided some insight into this behavior and these results are discussed.

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What this paper is about

An experimental program to measure the pumping speed of an Excalibur CVV2008 liquid helium cryosorption pump is described. Pumping speeds are reported for helium, hydrogen, and a 90% hydrogen –10% helium mixture in the pressure range 1×10−7–1×10−4 Torr. The helium pumping speed at 2×10−7 Torr was 3.2 l/s cm2, but decreased with loading to 1.6 l/s cm2 at 6×10−5 Torr. Attempts to operate at higher helium fluxes (Q≳8×10−5 sccm/s cm2) resulted in pressure and eventually thermal instabilities. The pumping speed of hydrogen at 5×10−7 Torr was 4.9 l/s cm2 and increased with pressure to 7.7 l/s cm2 at 5.5×10−6 Torr. For a 90% hydrogen–10% helium mixture, pumping speeds were inconsistent, varying between 1.4 and 5.6 l/s cm2. Residual gas analysis provided some insight into this behavior and these results are discussed.

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Available abstract

An experimental program to measure the pumping speed of an Excalibur CVV2008 liquid helium cryosorption pump is described. Pumping speeds are reported for helium, hydrogen, and a 90% hydrogen –10% helium mixture in the pressure range 1×10−7–1×10−4 Torr. The helium pumping speed at 2×10−7 Torr was 3.2 l/s cm2, but decreased with loading to 1.6 l/s cm2 at 6×10−5 Torr. Attempts to operate at higher helium fluxes (Q≳8×10−5 sccm/s cm2) resulted in pressure and eventually thermal instabilities. The pumping speed of hydrogen at 5×10−7 Torr was 4.9 l/s cm2 and increased with pressure to 7.7 l/s cm2 at 5.5×10−6 Torr. For a 90% hydrogen–10% helium mixture, pumping speeds were inconsistent, varying between 1.4 and 5.6 l/s cm2. Residual gas analysis provided some insight into this behavior and these results are discussed.

Key concepts: Torr, Helium, Hydrogen, Analytical Chemistry (journal), Liquid helium, Materials science, Atomic physics, Chemistry

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