1969Journal of Chromatographic ScienceRequires access

A Simple Device for Injecting a Sample From a Sealed Glass Tube Into a Gas Chromatograph

R. A. Back, N. J. Friswellt, J. Boden, J. M. Parsons

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Abstract

A simple device for injecting a sample from a sealed glass tube into a gas chromatograph is described. The sealed glass tube is equipped with a thin hemispheric break-seal of a special design, which is then fitted to the injector by a sliding O-ring seal. By a sliding motion of the sample tube, the break-seal is penetrated and shattered by a centrally mounted carrier gas inlet tube, and the sample is swept directly into the gas stream. The injector can be made of any convenient material; a metal-free, Teflon-and-glass design is described.

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What this paper is about

A simple device for injecting a sample from a sealed glass tube into a gas chromatograph is described. The sealed glass tube is equipped with a thin hemispheric break-seal of a special design, which is then fitted to the injector by a sliding O-ring seal. By a sliding motion of the sample tube, the break-seal is penetrated and shattered by a centrally mounted carrier gas inlet tube, and the sample is swept directly into the gas stream. The injector can be made of any convenient material; a metal-free, Teflon-and-glass design is described.

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Available abstract

A simple device for injecting a sample from a sealed glass tube into a gas chromatograph is described. The sealed glass tube is equipped with a thin hemispheric break-seal of a special design, which is then fitted to the injector by a sliding O-ring seal. By a sliding motion of the sample tube, the break-seal is penetrated and shattered by a centrally mounted carrier gas inlet tube, and the sample is swept directly into the gas stream. The injector can be made of any convenient material; a metal-free, Teflon-and-glass design is described.

Key concepts: Glass tube, Tube (container), Injector, Seal (emblem), Chemistry, Chromatography, Gas chromatography, Inlet

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