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2004•International Journal of Polymeric MaterialsRequires access

SYNTHESIS AND CHARACTERIZATION OF ETHYL ACRYLATE-METHYL ACRYLATE OLIGOMERS WITH A HYDROXYL END GROUP

Salomón R. Vásquez-García, R. Salgado-Delgado, J.A. Trejo-O'Reilly, Emanuel Ricardo Monteiro Martinez, Victor Manuel Castaño

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Abstract

A study on the method for the preparation of monohydroxyl functionalized oligomers has been performed using ethyl acrylate and methyl acrylate together with 2′2′ Azobisisobutyronitrile-AIBN (initiator), and 2-mercaptoethanol (2-MEOH) as functional chain-transfer agent. The estimation of the kinetics of the free radical chain polymerization by using statistical techniques is supported by the experimental studies. The oligomers compositions were determined by a quantitative analytical IR spectroscopic technique.

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A study on the method for the preparation of monohydroxyl functionalized oligomers has been performed using ethyl acrylate and methyl acrylate together with 2′2′ Azobisisobutyronitrile-AIBN (initiator), and 2-mercaptoethanol (2-MEOH) as functional chain-transfer agent. The estimation of the kinetics of the free radical chain polymerization by using statistical techniques is supported by the experimental studies. The oligomers compositions were determined by a quantitative analytical IR spectroscopic technique.

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Available abstract

A study on the method for the preparation of monohydroxyl functionalized oligomers has been performed using ethyl acrylate and methyl acrylate together with 2′2′ Azobisisobutyronitrile-AIBN (initiator), and 2-mercaptoethanol (2-MEOH) as functional chain-transfer agent. The estimation of the kinetics of the free radical chain polymerization by using statistical techniques is supported by the experimental studies. The oligomers compositions were determined by a quantitative analytical IR spectroscopic technique.

Key concepts: Azobisisobutyronitrile, Acrylate, Chemistry, Polymer chemistry, Methyl acrylate, Radical polymerization, Chain transfer, Radical initiator

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