Solid‐State NMR

Introduction Solid-state NMR Lineshapes The Orientational Dependence of the NMR Resonance Frequency Single-crystal NMR Powder Spectra One-dimensional 2H NMR Magic-angle Spinning CP MAS NMR 1H Solid-State NMR Recoupling Methods Heteronuclear Dipolar-coupled Spins: REDO Homonuclear Dipolar-coupled Spins The CSA: CODEX Homonuclear Two-dimensional Experiments Establishing the Backbone Connectivity in an Organic Molecule Dipolar-mediated Double-quantum Spectroscopy High-resolution 1H Solid-state NMR Anisotropic – Isotropic Correlation: The Measurement of CSAs The Investigation of Slow Dynamics: 2D Exchange 1H–1H DQ MAS Spinning-sideband Patterns Heteronuclear Two-dimensional Experiments Heteronuclear Correlation The Quantitative Determination of Heteronuclear Dipolar Couplings Torsional Angles Oriented Samples Half-integer Quadrupole Nuclei Summary