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OXYGEN IN BERYLLIUM

Silve Kallmann, Fred. Collier

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Abstract

The inert gas fusion method is shown to be well suited for the determination of the total O in Be metal. In order to release the oxygen from the very refractory beryllium oxide it is necessary to use a medium in which Be metal is soluble. Nickel was found to be the most suitable flux. Among the methods based on differential solubility of Be, the bromine-methanol procedure was found superior. A limitation of the method is caused by the unspecificity of the reagent. (Author)

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The inert gas fusion method is shown to be well suited for the determination of the total O in Be metal. In order to release the oxygen from the very refractory beryllium oxide it is necessary to use a medium in which Be metal is soluble. Nickel was found to be the most suitable flux. Among the methods based on differential solubility of Be, the bromine-methanol procedure was found superior. A limitation of the method is caused by the unspecificity of the reagent. (Author)

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Available abstract

The inert gas fusion method is shown to be well suited for the determination of the total O in Be metal. In order to release the oxygen from the very refractory beryllium oxide it is necessary to use a medium in which Be metal is soluble. Nickel was found to be the most suitable flux. Among the methods based on differential solubility of Be, the bromine-methanol procedure was found superior. A limitation of the method is caused by the unspecificity of the reagent. (Author)

Key concepts: Beryllium oxide, Bromine, Beryllium, Reagent, Solubility, Oxygen, Chemistry, Methanol

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